NMR spectroscopy explained : simplified theory, applications and examples for organic chemistry and structural biology /

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Autore principale: Jacobsen, Neil E.
Natura: Libro
Lingua:inglese
Pubblicazione: Hoboken, N.J. Wiley-Interscience 2007.
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Sommario:
  • Fundamentals of NMR spectroscopy in liquids
  • Interpretation of proton (p1sH) NMR spectra
  • NMR hardware and software
  • Carbon-13 (p13sC) NMR spectroscopy
  • NMR relaxation - inversion-recovery and the nuclear Overhauser effect (NOE)
  • The spin-echo and the attached proton test (APT)
  • Coherence transfer: INEPT and DEPT
  • Shaped pulses, pulsed field gradients and spin-locks: selective 1D NOE and 1D TOCSY
  • Two-dimensional NMR spectroscopy: HETCOR, COSY and TOCSY
  • Advanced NMR theory: NOESY and DQF-COSY
  • Inverse heteronuclear 2D experiments: HSQC, HMQC and HMBC
  • Biological NMR spectroscopy
  • Appendix A: A pictorial guide to NMR spin states
  • Appendix B: A survey of two-dimensional NMR experiments.