Graphene-wrapped sulfur/metal organic framework-derived microporous carbon composite for lithium sulfur batteries

A three-dimensional hierarchical sandwich-type graphene sheet-sulfur/carbon (GSS/CZIF8-D) composite for use in a cathode for a lithium sulfur (Li-S) battery has been prepared by an ultrasonic method. The microporous carbon host was prepared by a one-step pyrolysis of Zeolitic Imidazolate Framework-8...

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Autori principali: Chen, Renjie, Zhao, Teng, Tian, Tian, Cao, Shuai, Coxon, Paul, Xi, Kai, Fairen-Jimenez, David, Kumar, Ramachandran, Cheetham, Anthony
Altri autori: Organic Synthesis (ORSY)
Lingua:inglese
Pubblicazione: American Institute of Physics Publishing 2019
Accesso online:https://demo7.dspace.org/handle/123456789/446
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Riassunto:A three-dimensional hierarchical sandwich-type graphene sheet-sulfur/carbon (GSS/CZIF8-D) composite for use in a cathode for a lithium sulfur (Li-S) battery has been prepared by an ultrasonic method. The microporous carbon host was prepared by a one-step pyrolysis of Zeolitic Imidazolate Framework-8 (ZIF-8), a typical zinccontaining metal organic framework (MOF), which offers a tunable porous structure into which electro-active sulfur can be diffused. The thin graphene sheet, wrapped around the sulfur/zeolitic imidazolate framework-8 derived carbon (S/CZIF8-D) composite, has excellent electrical conductivity and mechanical flexibility, thus facilitating rapid electron transport and accommodating the changes in volume of the sulfur electrode. Compared with the S/CZIF8-D sample, Li-S batteries with the GSS/CZIF8-D composite cathode showed enhanced capacity, improved electrochemical stability, and relatively high columbic efficiency by taking advantage of the synergistic effects of the microporous carbon from ZIF-8 and a highly interconnected graphene network. Our results demonstrate that a porous MOF-derived scaffold with a wrapped graphene conductive network structure is a potentially efficient design for a battery electrode that can meet the challenge arising from low conductivity and volume change